Quantitative Organic Microanalysis

Quantitative Organic Microanalysis, Second Edition presents the recommendations of the American Chemical Society group for specification and methods of organic microanalysis. This book is organized into 23 chapters, and starts with discussions on test samples, blank tests, second type of efficient vibration-absorbing balance table, and microchemical balances. Other general topics covered include the Kjeldahl procedures to determine nitrogen compounds; oxygen flask combustions; determination of fluorine; and microhydrogenation. The final chapters present the modification of the procedure for the determination of oxygen using gravimetry. This book will be of great value to microanalysts, researchers, and college students who wants to expand their understanding in organic microanalysis. Content: Front Matter , Page iii Copyright , Page iv Dedication , Page v Preface to Second Edition , Pages vii-ix Foreword to First Edition , Page xi Acknowledgments , Pages xiii-xiv CHAPTER 1 - Introduction , Pages 1-29 CHAPTER 2 - The Microchemical Balance , Pages 30-49 CHAPTER 3 - Weighing on the Microchemical Balance , Pages 50-82 CHAPTER 4 - Preparation of Samples for Analysis , Pages 83-101 CHAPTER 5 - Standard Solutions (Microtitration Techniques) , Pages 102-132 CHAPTER 6 - Microdetermination of Metals by the Ashing Technique , Pages 133-150 CHAPTER 7 - Microdetermination of Nitrogen by the Dumas Method , Pages 151-187 CHAPTER 8 - Microdetermination of Nitrogen by the Kjeldahl Method , Pages 188-220 CHAPTER 9 - Microdetermination of Carbon and Hydrogen , Pages 221-275 CHAPTER 10 - Microdetermination of Sulfur , Pages 276-315 CHAPTER 11 - Microdetermination of Halogens , Pages 316-353 CHAPTER 12 - Microdetermination of Phosphorus , Pages 354-366 CHAPTER 13 - Microdetermination of Arsenic , Pages 367-376 CHAPTER 14 - Microdetermination of Oxygen , Pages 377-409 CHAPTER 15 - Microdetermination of Neutralization Equivalent, Ionic Hydrogen, or Carboxyl Groups , Pages 410-421 CHAPTER 16 - Microdetermination of Alkoxyl Groups (Methoxyl and Ethoxyl) , Pages 422-443 CHAPTER 17 - Microdetermination of Acyl Groups (Acetyl and Formyl) , Pages 444-453 CHAPTER 18 - Microdeterminations Carried Out on the Van Slyke Manometric Apparatus , Pages 454-494 CHAPTER 19 - Microdetermination of Unsaturation (Double Bonds)—Hydrogen Number , Pages 495-507 CHAPTER 20 - Microdetermination of Other Groups , Pages 508-527 CHAPTER 21 - Microdetermination of Molecular Weight , Pages 528-547 CHAPTER 22 - Microdetermination of Some Physical Constants , Pages 548-564 CHAPTER 23 - Calculations , Pages 565-602 AUTHOR INDEX , Pages 603-638 SUBJECT INDEX , Pages 639-665