NMR data interpretation explained - understanding 1D and 2D NMR spectra of organic compounds and natural products

Jacobsen Neil E. NMR data interpretation explained - understanding 1D and 2D NMR spectra of organic compounds and natural products 2017 [pdf 651sc 629c. 120.90mb] NMR Data Interpretation Explained shows how to get from an NMR spectrum to a chemical structure through numerous examples and exercises. Each topic is introduced with one or more examples of NMR data accompanied by detailed explanations of the interpretation of that data. Examples are then followed by a number of exercises using detailed images of NMR data. These are followed up by solutions, again with detailed explanations of the step-by-step reasoning used to solve the exercises. -- Abstract: NMR Data Interpretation Explained shows how to get from an NMR spectrum to a chemical structure through numerous examples and exercises. Each topic is introduced with one or more examples of NMR data accompanied by detailed explanations of the interpretation of that data. Examples are then followed by a number of exercises using detailed images of NMR data. These are followed up by solutions, again with detailed explanations of the step-by-step reasoning used to solve the exercises Through numerous examples, the principles of the relationship between chemical structure and the NMR spectrum are developed in a logical, step-by-step fashion Includes examples and exercises based on real NMR data including full 600 MHz one- and two-dimensional datasets of sugars, peptides, steroids and natural products Includes detailed solutions and explanations in the text for the numerous examples and problems and also provides large, very detailed and annotated sets of NMR data for use in understanding the material Describes both simple aspects of solution-state NMR of small molecules as well as more complex topics not usually covered in NMR books such as complex splitting patterns, weak long-range couplings, spreadsheet analysis of strong coupling patterns and resonance structure analysis for prediction of chemical shifts Advanced topics include all of the common two-dimensional experiments (COSY, ROESY, NOESY, TOCSY, HSQC, HMBC) covered strictly from the point of view of data interpretation, along with tips for parameter settings NMR Data Interpretation Explained shows how to get from an NMR spectrum to a chemical structure through numerous examples and exercises. Each topic is introduced with one or more examples of NMR data accompanied by detailed explanations of the interpretation of that data. Examples are then followed by a number of exercises using detailed images of NMR data. These are followed up by solutions, again with detailed explanations of the step-by-step reasoning used to solve the exercises. -- Read more... Abstract: NMR Data Interpretation Explained shows how to get from an NMR spectrum to a chemical structure through numerous examples and exercises. Each topic is introduced with one or more examples of NMR data accompanied by detailed explanations of the interpretation of that data. Examples are then followed by a number of exercises using detailed images of NMR data. These are followed up by solutions, again with detailed explanations of the step-by-step reasoning used to solve the exercises NMR Data Interpretation Explained shows how to get from an NMR spectrum to a chemical structure through numerous examples and exercises. Each topic is introduced with one or more examples of NMR data accompanied by detailed explanations of the interpretation of that data. Examples are then followed by a number of exercises using detailed images of NMR data. These are followed up by solutions, again with detailed explanations of the step-by-step reasoning used to solve the exercises. -- Back cover Content: Spectroscopy and the Proton NMR Experiment -- Chemical Shifts and Splitting Patterns -- Proton (1H) NMR of Aromatic Compounds -- Carbon-13 (13C) NMR -- Alkenes (Olefins) -- Chirality and Stereochemistry: Natural Products -- Selective Proton Experiments: Biological Molecules -- Homonuclear Two-Dimensional NMR: Correlation of One Hydrogen (1H) to Another -- Heteronuclear Two-Dimensional NMR: Correlation of One Hydrogen (1H) to One Carbon (13C) -- Structure Elucidation Using 2D NMR.