بازاریابی وابسته و آمازون FBA (2 کتاب در 1): بازاریابی وابسته و تجارت آمازون FBA را در 5 روز بیاموزید و آن را به خوبی یاد بگیرید (کسب و کار آنلاین آسان شده است)

Gilbert John C. Experimental Organic Chemistry - A Miniscale and Microscale Approach 6 ed. 2016 [pdf 968sc 931+2c. 36.15mb] Contents in Brief Table of Contents Ch 1: Introduction, Record Keeping, and Laboratory Safety 1.1: Introduction 1.2: Preparing for the Laboratory 1.3: Working in the Laboratory 1.4: The Laboratory Notebook 1.5: General Protocol for the Laboratory Notebook 1.6: Types of Organic Experiments and Notebook Formats 1.7: Sample Calculations for Notebook Records 1.8: Safe Laboratory Practice: Overview 1.9: Safety: General Discussion 1.10: Safety: Material Safety Data Sheets (MSDSs) 1.11: Safety: Disposal of Chemicals Ch 2: Techniques and Apparatus 2.1: Glassware: Precautions and Cleaning 2.2: Standard-Taper Glassware for Miniscale Procedures 2.3: Standard-Taper Glassware for Microscale Procedures 2.4: Assembling Apparatus 2.5: Measuring and Transferring Liquids 2.6: Weighing Methods 2.7: Melting-Point Methods and Apparatus 2.8: Boiling-Point Methods and Apparatus 2.9: Heating Methods 2.10: Cooling Techniques 2.11: Stirring Methods 2.12: Centrifugation 2.13: Simple Distillation 2.14: Fractional Distillation 2.15: Vacuum Distillation 2.16: Steam Distillation 2.17: Filtration Apparatus and Techniques 2.18: Decolorizing Carbon 2.19: Decanting Solutions 2.20: Sublimation 2.21: Extraction 2.22: Heating under Reflux 2.23: Gas Traps 2.24: Drying Agents 2.25: Drying Organic Solutions 2.26: Drying Solids 2.27: Drying Tubes 2.28: Drying Apparatus 2.29: Evaporating Solvents Ch 3: Solids: Recrystallization and Melting Points 3.1: Introduction 3.2: Recrystallization 3.3: Physical Constants: Melting Points Ch 4: Liquids: Distillation and Boiling Points 4.1: Introduction 4.2: Boiling Points of Pure Liquids 4.3: Simple Distillation 4.4: Fractional Distillation 4.5: Steam Distillation 4.6: Steam Distillation: Isolation of Citral from Lemon Grass Oil 4.7: Qualitative Analysis Ch 5: Extraction 5.1: Introduction 5.2: Theory of Extraction 5.3: Base and Acid Extractions 5.4: Extraction of a Natural Product: Trimyristin Ch 6: Chromatography 6.1: Introduction 6.2: Thin-Layer Chromatography 6.3: Column Chromatography 6.4: Gas-Liquid Chromatography Ch 7: Stereoisomers 7.1: Introduction 7.2: Separation of Diastereomeric 1,2-Cyclohexanediols 7.3: Isomerization of Dimethyl Maleate to Dimethyl Fumarate 7.4: Properties of the Enantiomers of Carvone 7.5: Polarimetry 7.6: Resolution of Racemic 1-Phenylethanamine Ch 8: Spectral Methods 8.1: Introduction 8.2: Infrared (IR) Spectroscopy 8.3: Nuclear Magnetic Resonance (NMR) Spectroscopy 8.4: Ultraviolet and Visible Spectroscopy 8.5: Mass Spectrometry Ch 9: Alkanes 9.1: Introduction 9.2: Chlorination Using Sulfuryl Chloride 9.3: Bromination: Selectivity of Hydrogen Atom Abstraction Ch 10: Alkenes 10.1: Introduction 10.2: Dehydrohalogenation of Alkyl Halides 10.3: Dehydration of Alcohols 10.4: Addition Reactions of Alkenes: Overview 10.5: Addition of Hydrobromic Acid to Alkenes 10.6: Bromination of Alkenes 10.7: Acid-Catalyzed Hydration of Alkenes 10.8: Hydroboration-Oxidation of Alkenes Ch 11: Alkynes 11.1: Introduction 11.2: Dehydrohalogenation of 1,2-Dihaloalkanes 11.3: Addition Reactions of Alkynes 11.4: Terminal Alkynes as Acids Ch 12: Dienes: The Diels-Alder Reaction 12.1: Introduction 12.2: Mechanistic and Stereochemical Aspects 12.3: Applications of Diels-Alder Reactions Ch 13: Kinetic and Thermodynamic Control of a Reaction 13.1: Introduction 13.2: Formation of Semicarbazones under Kinetic and Thermodynamic Control Ch 14: Nucleophilic Aliphatic Substitution: Preparation of Alkyl Halides 14.1: General Concepts 14.2: Classification of Nucleophilic Substitution Reactions 14.3: Competition between Substitution and Elimination 14.4: Preparation of 1-Bromobutane: An SN2 Reaction 14.5: Preparation of 2-Chloro-2-Methylbutane: An SN1 Reaction 14.6: Chemical Kinetics: Evidence for Nucleophilic Substitution Mechanisms 14.7: Competing Nucleophiles in SN Reactions 14.8: Competition between Substitution and Elimination Ch 15: Electrophilic Aromatic Substitution 15.1: Introduction 15.2: Friedel-Crafts Alkylation of p-Xylene with 1-Bromopropane 15.3: Friedel-Crafts Acylation of Anisole 15.4: Nitration of Bromobenzene 15.5: Substituent Effects on Electrophilic Aromatic Substitution 15.6: Azo Dyes and the Chemistry of Dyeing Fabrics Ch 16: Oxidation of Alcohols and Carbonyl Compounds 16.1: Introduction 16.2: Preparation of Aldehydes and Ketones by Oxidation of Alcohols 16.3: Base-Catalyzed Oxidation-Reduction of Aldehydes: The Cannizzaro Reaction Ch 17: Reduction Reactions of Double Bonds: Alkenes, Carbonyl Compounds, and Imines 17.1: Introduction 17.2: Catalytic Hydrogenation of the Carbon-Carbon Double Bond 17.3: Reduction of Imines; Preparation of Amines 17.4: Reduction of Carbonyl Compounds; Preparation of Alcohols 17.5: Enantioselective Reductions: A Chiral Alcohol from a Ketone 17.6: Determining Optical Purity Ch 18: Reactions of Carbonyl Compounds 18.1: Introduction 18.2: The Wittig and Related Reactions 18.3: Reactions of Stabilized Carbanions from Carbonyl Compounds 18.4: Conjugate Addition to an a,b-Unsaturated Ketone 18.5: Heterocyclic Compounds: Synthesis of a 1,2,3,4-Tetrahydropyrimidine-2-One Ch 19: Organometallic Chemistry 19.1: Introduction 19.2: Grignard Reagents: Preparation 19.3: Grignard Reagents: Reactions 19.4: Special Experimental Techniques 19.5: Organozinc Reagents: Preparation and Reaction 19.6: Transition Metal Catalyzed Reactions and Procedure for Suzuki Reaction Ch 20: Carboxylic Acids and Their Derivatives 20.1: Introduction 20.2: Esters and the Fischer Esterification 20.3: Amides and Insect Repellents 20.4: Amides and Chemiluminescence Ch 21: Multistep Organic Synthesis 21.1: Introduction 21.2: Sulfanilamide: Discovery and Synthesis of the First Antibiotic 21.3: Synthesis of 1-Bromo-3-Chloro-5-Iodobenzene 21.4: Lidocaine: Synthesis of an Anesthetic Agent Ch 22: Polymers 22.1: Introduction 22.2: Chain-Reaction Polymerization 22.3: Step-Growth Polymerization Ch 23: Carbohydrates 23.1: Introduction 23.2: Monosaccharides: General Principles 23.3: Disaccharides: Hydrolysis of Sucrose 23.4: Carbohydrates: Their Characterization and Identification Ch 24: a-Amino Acids and Peptides 24.1: Introduction 24.2: Synthesis of Peptides and Polypeptides 24.3: Synthesis of the Protected Dipeptide Ala-Phe-OMe Index Helps you perform chemistry experiments with skill and confidence in your organic chemistry lab course. This lab manual first covers equipment, record keeping, and safety in the laboratory, then walks you step by step through the laboratory techniques you'll need to perform all experiments.