عملیات و ایمنی کارخانه‌های پایلوت دانشگاهی و صنعتی [این جلد به منظور به اشتراک گذاشتن مقالات ارائه‌شده در نشست ملی ۲۴۵ ام ACS، که از ۷ تا ۱۲ آوریل ۲۰۱۳ در نیواورلئان، لوئیزیانا برگزار شد، توسعه یافته است]

This symposium series volume was developed in order to share papers presented at the 245th ACS National Meeting on the topic of pilot plants. The Industrial and Chemical Engineering, Applied Chemical Technology Subdivision hosted a one-day symposium for industry and academic researchers to present and share their work and best practices on operations and safety in pilot plant environments. Designing and building "pilot plants" can be a big challenge, and this volume outlines the proper operations needed to run a plant safely, in both academic and industrial environments. The book addresses issues like chemical separation, chemical reactions, waste generation, process controls, and spatial considerations, as well as safety precautions. It describes ways in which plant designers and contractors can consider ease of operation, maintenance, pinch-points, and sampling, among other aspects. In contrast to workers in large-scale facilities, pilot plant workers in both industry and academia are not only exposed to hazardous substances, they are exposed to such materials in a smaller setting and thus to potentially greater concentrations. This book brings together workers and researchers in pilot plant environments to present and share their best practices as regards operations and safety title 1 preface 6 1 - Academia and Industrial Pilot Plant Operations and Safety 8 2 - Thermodynamics as a Tool for Laboratory and Chemical Safety in the Undergraduate Chemistry Curriculum 31 3 - Considerations for Scale-Up – Moving from the Bench to the Pilot Plant to Full Production 42 4 - Management of Change: Pilot Plant Scale 51 5 - Transitioning Culture: Teaching and Modeling Workplace Behavior 57 6 - Blast Energy and Damage Assessment from the Mechanical Explosion of Compressed Gas Cylinders 63 7 - A Practical Method of Neutralizing Cr(VI) in Phillips Polymerization Catalysts 76 8 - Scale Up in Brewing: Factors in Changing Batch Size from 5 Gallons to 15 Barrels 87 index 93 Content: Academia and industrial pilot plant operations and safetyThermodynamics as a tool for laboratory and chemical safety in the undergraduate chemistry curriculum -- Considerations for scale-up : moving from the bench to the pilot plant to full production -- Management of change : pilot plant scale -- Transitioning culture : teaching and modeling workplace behavior -- Blast energy and damage assessment from the mechanical explosion of compressed gas cylinders -- A practical method of neutralizing Cr(VI) in Phillips polymerization catalysts -- Scale up in brewing : factors in changing batch size from 5 gallons to 15 barrels. An ACS Symposium Series book on best practices and safety considerations for setting up a chemical "pilot plant," in both environmental and academic environments.